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{{orphan|date=December 2008}} |
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{{chembox |
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{{chembox |
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| verifiedrevid = 413095043 |
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| Name = 2,2'-Dipyridyldisulfide |
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| Name = 2,2′-Dipyridyldisulfide |
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| ImageFile = 2,2'-Dipyridyldisulfide.svg |
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| ImageFile = 2,2'-Dipyridyldisulfide.svg |
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| ImageAlt = Skeletal formula of DPS |
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<!-- | ImageSize = 188px --> |
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| IUPACName = 2,2'-Dipyridyldisulfide |
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| ImageFile1 = 2,2'-Dipyridyldisulfide-3D-spacefill.png |
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| ImageAlt1 = Space-filling model of the DPS molecule |
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| OtherNames = 2,2'-Dipyridyldisulphide<br />Aldrithiol-2 |
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| PIN = 2,2′-Disulfanediyldipyridine |
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| OtherNames = 1,2-Di(pyridin-2-yl)disulfane (not recommended)<br />2,2′-Dipyridyldisulfide<br />2,2′-Dipyridyldisulphide<br />Aldrithiol-2 |
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| Section1 = {{Chembox Identifiers |
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| Section1 = {{Chembox Identifiers |
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| ChemSpiderID_Ref = {{chemspidercite|correct|chemspider}} |
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| ChemSpiderID = 58603 |
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| ChemSpiderID = 58603 |
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| InChI = 1/C10H8N2S2/c1-3-7-11-9(5-1)13-14-10-6-2-4-8-12-10/h1-8H |
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| InChI = 1/C10H8N2S2/c1-3-7-11-9(5-1)13-14-10-6-2-4-8-12-10/h1-8H |
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| InChIKey = HAXFWIACAGNFHA-UHFFFAOYAJ |
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| InChIKey = HAXFWIACAGNFHA-UHFFFAOYAJ |
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| SMILES1 = c1ccnc(c1)SSc2ccccn2 |
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| SMILES1 = c1ccnc(c1)SSc2ccccn2 |
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| ChEMBL_Ref = {{ebicite|correct|EBI}} |
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| ChEBI = 143170 |
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| ChEMBL = 118678 |
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| ChEMBL = 118678 |
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| PubChem = 65093 |
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| EC_number = 218-343-1 |
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| StdInChI_Ref = {{stdinchicite|correct|chemspider}} |
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| StdInChI = 1S/C10H8N2S2/c1-3-7-11-9(5-1)13-14-10-6-2-4-8-12-10/h1-8H |
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| StdInChI = 1S/C10H8N2S2/c1-3-7-11-9(5-1)13-14-10-6-2-4-8-12-10/h1-8H |
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| StdInChIKey_Ref = {{stdinchicite|correct|chemspider}} |
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| StdInChIKey = HAXFWIACAGNFHA-UHFFFAOYSA-N |
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| StdInChIKey = HAXFWIACAGNFHA-UHFFFAOYSA-N |
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| CASNo = 2127-03-9 |
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| CASNo = 2127-03-9 |
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| UNII_Ref = {{fdacite|correct|FDA}} |
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| UNII = L6X912UPBU |
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| SMILES = S(Sc1ncccc1)c2ncccc2 |
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| SMILES = S(Sc1ncccc1)c2ncccc2 |
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| Formula = |C=10|H=8|N=2|S=2 |
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| Formula = |C=10|H=8|N=2|S=2 |
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| MolarMass = |
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| MolarMass = |
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| MeltingPtCL= 56 |
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| MeltingPtC = 56 to 58 |
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| MeltingPtCH = 58 |
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}} |
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}} |
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| Section7 = {{Chembox Hazards |
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| Section7 = {{Chembox Hazards |
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| MainHazards = Irritant ('''Xi''') |
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| MainHazards = Irritant ('''Xi''') |
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| RPhrases = {{R36/37/38}} |
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| GHSPictograms = {{GHS07}} |
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| GHSSignalWord = Warning |
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| SPhrases = {{S36/37/39}} |
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| HPhrases = {{H-phrases|315|319|335}} |
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| PPhrases = {{P-phrases|261|264|271|280|302+352|304+340|305+351+338|312|321|332+313|337+313|362|403+233|405|501}} |
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'''2,2'-Dipyridyldisulfide''', sometimes known as DPS, is used for preparing thiols<ref>{{cite journal | author = Futaki S. and Kitagawa K. | title = Peptide-Unit Assembling Using Disulfide Cross-Linking - a New Approach for Construction of Protein Models | year = 1994 | journal = ] | volume = 35 | issue = 8 | pages = 1267–1270 | doi=10.1016/0040-4039(94)88040-9}}</ref><ref>{{cite journal | journal = ] | title = Special Reagents for Thiol Groups | volume = 4 | issue = 3 | pages = 33–46}}</ref> and activating or protecting ] with ] in the following reaction.<ref>{{cite journal | journal = ] | author = Thalmann A., Oertle K. and Gerlach H | title = Synthesis of ricinelaidic acid lactone| volume = 7 | pages = 470}}</ref> |
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'''2,2′-Dipyridyldisulfide''', sometimes known as DPS, is used for preparing thiols<ref>{{cite journal | author = Futaki S. and Kitagawa K. | title = Peptide-Unit Assembling Using Disulfide Cross-Linking - a New Approach for Construction of Protein Models | year = 1994 | journal = ] | volume = 35 | issue = 8 | pages = 1267–1270 | doi=10.1016/0040-4039(94)88040-9}}</ref><ref>{{cite journal | journal = ] | title = Special Reagents for Thiol Groups | volume = 4 | issue = 3 | pages = 33–46}}</ref> and activating ] for ]s, as in the following reaction:<ref>{{cite journal | journal = ] | author = Thalmann A., Oertle K. and Gerlach H | title = Ricinelaidic acid lactone| year = 1985 | volume = 7 | pages = 470 |doi= 10.15227/orgsyn.063.0192}}</ref> |
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==Uses== |
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==Uses== |
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It is also used in molecular biology as an ], for example to oxidise free thiols to form disulfide bonds in proteins. |
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It is also used in molecular biology as an ], for example to oxidise free ]s to form ]s in proteins. |
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==References== |
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==References== |
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{{DEFAULTSORT:Dipyridyldisulfide, 2,2'-}} |
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{{DEFAULTSORT:Dipyridyldisulfide, 2,2'-}} |
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